methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

Base Information

Chemical Name:methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside
CAS No.:880480-61-5
Molecular Formula:C₅₈H₆₄O₁₃
Molecular Weight:969.138
Hs Code.:

Synonyms:methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

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Technology Process of methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

There total 3 articles about methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.2%

: 880480-39-7
1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl fluoride

: 880480-57-9
2-O-methoxymethyl 3,4,5-tri-O-benzyl-β-D-fructopyranoside

: 880480-61-5
methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

Guidance literature:: With 4 A molecular sieve; zirconocene dichloride; silver perchlorate; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.3987/COM-05-S(K)54

Reference yield:

: 880480-38-6
1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranose

: 880480-61-5
methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 81.8 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 1 h / 20 °C

2: 57.2 percent / zirconocene dichloride; 4 Angstroem molecular sieves; AgClO₄ / CH₂Cl₂ / 2.5 h / 20 °C

With diethylamino-sulfur trifluoride; 4 A molecular sieve; zirconocene dichloride; silver perchlorate; In dichloromethane;
DOI:10.3987/COM-05-S(K)54

Reference yield:

: 880480-55-7
methoxymethyl 1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranoside

: 880480-61-5
methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaOMe / methanol / 2 h / 20 °C

2: 57.2 percent / zirconocene dichloride; 4 Angstroem molecular sieves; AgClO₄ / CH₂Cl₂ / 2.5 h / 20 °C

With 4 A molecular sieve; zirconocene dichloride; sodium methylate; silver perchlorate; In methanol; dichloromethane;
DOI:10.3987/COM-05-S(K)54