C₄₇H₇₂N₂O₁₄Si

Base Information

Chemical Name:C₄₇H₇₂N₂O₁₄Si
CAS No.:925451-91-8
Molecular Formula:C₄₇H₇₂N₂O₁₄Si
Molecular Weight:917.179
Hs Code.:

C<sub>47</sub>H<sub>72</sub>N<sub>2</sub>O<sub>14</sub>Si

Synonyms:C₄₇H₇₂N₂O₁₄Si

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Chemical Property of C₄₇H₇₂N₂O₁₄Si

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Technology Process of C₄₇H₇₂N₂O₁₄Si

There total 5 articles about C₄₇H₇₂N₂O₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874758-58-4
3-acetoxymethyl-8-allyloxy-1-(3-tert-butoxycarbonyl-2,2-dimethyl-oxazolidin-4-yl)-7-methoxy-6-methyl-3,4-dihydro-1H-isoquinoline-2-carboxylic acid allyl ester

: 925451-91-8
C₄₇H₇₂N₂O₁₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / CeCl₃*7H₂O; oxalic acid / acetonitrile / 2 h / 20 °C

2: oxalyl chloride; dimethylsulfoxide; triethylamine / CH₂Cl₂ / -60 - 20 °C

3: 74 percent / CH₃MgCl / tetrahydrofuran; CH₂Cl₂ / 20 °C

4: 88 percent / DIPEA / CHCl₃ / 6 h / 20 - 60 °C

With cerium(III) chloride; oxalyl dichloride; methylmagnesium chloride; oxalic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; chloroform; acetonitrile; 2: Swern oxidation;
DOI:10.1002/anie.200603179

Reference yield:

: 925451-73-6
C₁₇H₃₀O₄Si

: 925451-91-8
C₄₇H₇₂N₂O₁₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / trimethylsilyl bromide / CH₂Cl₂ / -20 - 10 °C

2: 74 percent / CH₃MgCl / tetrahydrofuran; CH₂Cl₂ / 20 °C

3: 88 percent / DIPEA / CHCl₃ / 6 h / 20 - 60 °C

With trimethylsilyl bromide; methylmagnesium chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1002/anie.200603179

Reference yield:

: 925451-75-8
C₂₈H₄₀N₂O₉

: 925451-91-8
C₄₇H₇₂N₂O₁₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride; dimethylsulfoxide; triethylamine / CH₂Cl₂ / -60 - 20 °C

2: 74 percent / CH₃MgCl / tetrahydrofuran; CH₂Cl₂ / 20 °C

3: 88 percent / DIPEA / CHCl₃ / 6 h / 20 - 60 °C

With oxalyl dichloride; methylmagnesium chloride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; chloroform; 1: Swern oxidation;
DOI:10.1002/anie.200603179