2-CHLORO-4-NITROTHIOBENZAMIDE

Base Information

• Chemical Name: 2-CHLORO-4-NITROTHIOBENZAMIDE
• CAS No.: 1233509-74-4
• Molecular Formula: C₇H₅ClN₂O₂S
• Molecular Weight: 216.648
• Mol file: 1233509-74-4.mol

Synonyms:C₇H₅ClN₂O₂S

Chemical Property of 2-CHLORO-4-NITROTHIOBENZAMIDE

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

2-Chloro-4-nitrothiobenzamide 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-CHLORO-4-NITROTHIOBENZAMIDE

There total 3 articles about 2-CHLORO-4-NITROTHIOBENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Novastat (3011-89-0) → C7H5ClN2O2S (1233509-74-4)

Guidance literature:

With Lawessons reagent; In tetrahydrofuran; Reflux;

DOI:10.1016/j.bmcl.2012.12.065

Reference yield:

2-chloro-4-nitrobenzoic acid (99-60-5) → C7H5ClN2O2S (1233509-74-4)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / chloroform / 8 h / Reflux

2: ammonium hydroxide / tetrahydrofuran / 2 h / 20 °C

3: Lawessons reagent / tetrahydrofuran / Reflux

With Lawessons reagent; ammonium hydroxide; thionyl chloride; In tetrahydrofuran; chloroform;

DOI:10.1016/j.bmcl.2012.12.065

Reference yield:

2-chloro-4-nitrobenzoyl chloride (7073-36-1) → C7H5ClN2O2S (1233509-74-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium hydroxide / tetrahydrofuran / 2 h / 20 °C

2: Lawessons reagent / tetrahydrofuran / Reflux

With Lawessons reagent; ammonium hydroxide; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2012.12.065

upstream raw materials:

Novastat

2-chloro-4-nitrobenzoic acid

2-chloro-4-nitrobenzoyl chloride

Downstream raw materials:

C₈H₃ClN₂O₃S₂

Refernces