1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate

Base Information

Chemical Name:1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate
CAS No.:1415236-32-6
Molecular Formula:C₂₁H₃₀N₂O₆
Molecular Weight:406.479
Hs Code.:

Synonyms:1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate

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Chemical Property of 1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate

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Technology Process of 1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate

There total 2 articles about 1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5153-67-3
nitrostyrene

: 1259065-07-0
1-tert-butyl 4-methyl azepane-1,4-dicarboxylate

: 1415236-32-6
1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexanes; at -78 - 20 ℃; for 0.666667h;

Reference yield:

: 868284-36-0
(rac)-1-(tert-butoxycarbonyl)azepane-4-carboxylic acid

: 1415236-32-6
1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

2: diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.67 h / -78 - 20 °C

With n-butyllithium; diisopropylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexanes; dichloromethane;

Reference yield:

: 1415236-32-6
1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate

: 1415236-35-9
tert-butyl 1-oxo-4-phenyl-2,8-diazaspiro[4.6]undecane-8-carboxylate

Guidance literature:: 1-tert-butyl 4-methyl 4-(2-nitro-1-phenylethyl)azepane-1,4-dicarboxylate; With sodium tetrahydroborate; ethanol; nickel dichloride; In methanol; at 20 ℃; for 1h;

With ammonia; In methanol; ethyl acetate;