6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane

Base Information

Chemical Name:6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane
CAS No.:1429638-35-6
Molecular Formula:C₃₀H₄₈O₄Si₂
Molecular Weight:528.88
Hs Code.:

Synonyms:6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane

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Chemical Property of 6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane

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Technology Process of 6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane

There total 4 articles about 6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1429638-34-5
10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecan-6-ol

: 69739-34-0
t-butyldimethylsiyl triflate

: 1429638-35-6
6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1021/ol4005799

Reference yield:

: 172843-09-3
1-O-(tert-butyldiphenylsilyl)-1,3-dihydroxy-2-propanone

: 1429638-35-6
6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

2: tetrahydrofuran / 0.5 h / -78 - 20 °C / Inert atmosphere

3: pyridine / dichloromethane / 72 h / 20 °C / Inert atmosphere

With pyridine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol4005799

Reference yield:

: 1429638-33-4
1-(tert-butyldiphenylsilyloxy)-3-methoxymethoxypropan-2-one

: 1429638-35-6
6-(tert-butyldimethylsilyloxy)-10,10-dimethyl-9,9-diphenyl-6-(prop-1-en-2-yl)-2,4,8-trioxa-9-silaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.5 h / -78 - 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 72 h / 20 °C / Inert atmosphere

With pyridine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol4005799