benzyl 6β-<-N-(2,2,2-trichloroethoxycarbonyl)-N-trifluoromethylsulphonylamino>penicillanate 1α-oxide

Base Information Edit

Chemical Name:benzyl 6β-<-N-(2,2,2-trichloroethoxycarbonyl)-N-trifluoromethylsulphonylamino>penicillanate 1α-oxide
CAS No.:93521-26-7
Molecular Formula:C₁₉H₁₈Cl₃F₃N₂O₈S₂
Molecular Weight:629.847
Hs Code.:
Mol file:93521-26-7.mol

Synonyms:benzyl 6β-<-N-(2,2,2-trichloroethoxycarbonyl)-N-trifluoromethylsulphonylamino>penicillanate 1α-oxide

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Chemical Property of benzyl 6β-<-N-(2,2,2-trichloroethoxycarbonyl)-N-trifluoromethylsulphonylamino>penicillanate 1α-oxide Edit

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Technology Process of benzyl 6β-<-N-(2,2,2-trichloroethoxycarbonyl)-N-trifluoromethylsulphonylamino>penicillanate 1α-oxide

There total 2 articles about benzyl 6β-<-N-(2,2,2-trichloroethoxycarbonyl)-N-trifluoromethylsulphonylamino>penicillanate 1α-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 93521-25-6
benzyl 6β-penicillanate

: 93521-26-7
benzyl 6β-<-N-(2,2,2-trichloroethoxycarbonyl)-N-trifluoromethylsulphonylamino>penicillanate 1α-oxide

Guidance literature:: With peracetic acid; In dichloromethane; 1) -10 deg C 2) 0 deg C, 16 h;

Reference yield:

: 82954-45-8
benzyl 6β-(N-trifluoromethylsulphonylamino)penicillanate

: 93521-26-7
benzyl 6β-<-N-(2,2,2-trichloroethoxycarbonyl)-N-trifluoromethylsulphonylamino>penicillanate 1α-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / triethylamine, 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / 0 °C

2: 83 percent / 5.24percent peracetic acid in AcOH / CH₂Cl₂ / 1) -10 deg C 2) 0 deg C, 16 h

With peracetic acid; dmap; triethylamine; In dichloromethane;