Benzhydryl-<4-chlor-benzyliden>-aminoxyd

Base Information

• Chemical Name: Benzhydryl-<4-chlor-benzyliden>-aminoxyd
• CAS No.: 99672-90-9
• Molecular Formula: C₂₀H₁₆ClNO
• Molecular Weight: 321.806

Synonyms:Benzhydryl-<4-chlor-benzyliden>-aminoxyd

Chemical Property of Benzhydryl-<4-chlor-benzyliden>-aminoxyd

Chemical Property:

Purity/Quality:

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Technology Process of Benzhydryl-<4-chlor-benzyliden>-aminoxyd

There total 1 articles about Benzhydryl-<4-chlor-benzyliden>-aminoxyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzophenone oxime (574-66-3) + 1-Chloro-4-(chloromethyl)benzene (104-83-6) → Benzophenon- (94579-46-1) + Benzhydryl-<4-chlor-benzyliden>-aminoxyd (99672-90-9)

Guidance literature:

Multistep reaction; (i) EtONa, EtOH, (ii) /BRN= 471558/;

DOI:10.1021/ja00866a027

Reference yield: 42.0%

2-methylpropenal (78-85-3,25120-30-3) + Benzhydryl-<4-chlor-benzyliden>-aminoxyd (99672-90-9) → (3R,4R)-3-(4-chlorophenyl)-2-diphenylmethyl-4-formyl-4-methylisoxazolidine

Guidance literature:

With C₅₀H₃₄F₁₂O₇Ti₂; In dichloromethane; at 0 ℃; for 24h; optical yield given as %ee;

DOI:10.1039/b804987d

Reference yield:

2-methylpropenal (78-85-3,25120-30-3) + Benzhydryl-<4-chlor-benzyliden>-aminoxyd (99672-90-9) → (3R,4R)-3-(4-chlorophenyl)-2-diphenylmethyl-4-formyl-4-methylisoxazolidine + (3S,4S)-3-(4-chlorophenyl)-2-diphenylmethyl-4-formyl-4-methylisoxazolidine

Guidance literature:

With C₄₆H₃₄I₄O₇Ti₂; In dichloromethane; at 0 ℃; for 24h; optical yield given as %ee;

DOI:10.1039/b804987d

upstream raw materials:

Benzophenone oxime

1-Chloro-4-(chloromethyl)benzene

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