N,N-bis[3-(4-bromophenyl)prop-2-ynyl]-2-(6-methoxyhex-4-ynyloxy)benzenamine

Base Information

Chemical Name:N,N-bis[3-(4-bromophenyl)prop-2-ynyl]-2-(6-methoxyhex-4-ynyloxy)benzenamine
CAS No.:1186029-64-0
Molecular Formula:C₃₁H₂₇Br₂NO₂
Molecular Weight:605.369
Hs Code.:

Synonyms:N,N-bis[3-(4-bromophenyl)prop-2-ynyl]-2-(6-methoxyhex-4-ynyloxy)benzenamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis[3-(4-bromophenyl)prop-2-ynyl]-2-(6-methoxyhex-4-ynyloxy)benzenamine

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Technology Process of N,N-bis[3-(4-bromophenyl)prop-2-ynyl]-2-(6-methoxyhex-4-ynyloxy)benzenamine

There total 1 articles about N,N-bis[3-(4-bromophenyl)prop-2-ynyl]-2-(6-methoxyhex-4-ynyloxy)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 589-87-7
1,4-bromoiodobenzene

: 1186029-81-1
C₁₉H₂₁NO₂

: 1186029-64-0
N,N-bis[3-(4-bromophenyl)prop-2-ynyl]-2-(6-methoxyhex-4-ynyloxy)benzenamine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol9014893

Reference yield: 95.0%

: 1186029-64-0
N,N-bis[3-(4-bromophenyl)prop-2-ynyl]-2-(6-methoxyhex-4-ynyloxy)benzenamine

: C₃₁H₂₇Br₂NO₂

Guidance literature:: With 1,2-bis[(2S,5S)-2,5-dimethylphospholano]benzene(cyclooctadiene)rhodium(I) trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 80 ℃; for 0.5h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol9014893