1-Iodo-4-methoxy-2,3-dimethylbenzene

Base Information

• Chemical Name: 1-Iodo-4-methoxy-2,3-dimethylbenzene
• CAS No.: 17938-70-4
• Molecular Formula: C9H11 I O
• Molecular Weight: 262.09
• DSSTox Substance ID: DTXSID50556022
• Nikkaji Number: J701.828B
• Wikidata: Q82437488
• Mol file: 17938-70-4.mol

Synonyms:1-Iodo-4-methoxy-2,3-dimethylbenzene;17938-70-4;1-IODO-2,3-DIMETHYL-4-METHOXYBENZENE;4-Methoxy-2,3-dimethyliodobenzene;Benzene, 1-iodo-4-methoxy-2,3-dimethyl-;MFCD07779020;4-Iodo-2,3-dimethylanisole;SCHEMBL16313227;DTXSID50556022;2,3-dimethyl-4-methoxyiodobenzene;CL9081;AKOS015910363;AM83246;SY033645;CS-0153604;1-Iodo-4-methoxy-2 pound not3-dimethylbenzene;A881252

Chemical Property of 1-Iodo-4-methoxy-2,3-dimethylbenzene

Chemical Property:

• PSA: 9.23000
• LogP: 2.91660
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 261.98546
• Heavy Atom Count: 11
• Complexity: 127

Purity/Quality:

97% ^*data from raw suppliers

1-Iodo-4-methoxy-2,3-dimethylbenzene >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1C)I)OC

Technology Process of 1-Iodo-4-methoxy-2,3-dimethylbenzene

There total 5 articles about 1-Iodo-4-methoxy-2,3-dimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2,3-dimethylanisole (2944-49-2) → 1-iodo-4-methoxy-2,3-dimethylbenzene (17938-70-4)

Guidance literature:

With N,N,N-trimethylbenzenemethanaminium dichloroiodate; zinc(II) chloride; In acetic acid; for 0.5h; Ambient temperature;

DOI:10.1246/cl.1988.795

Reference yield: 47.0%

2,3-dimethyl-4-methoxyaniline (77375-19-0) → 1-iodo-4-methoxy-2,3-dimethylbenzene (17938-70-4)

Guidance literature:

With sulfuric acid; potassium iodide; sodium nitrite;

DOI:10.1002/adsc.200800421

Reference yield: 33.0%

2,3-dimethylanisole (2944-49-2) → 1-iodo-4-methoxy-2,3-dimethylbenzene (17938-70-4) + 2,4-Diiodo-3-methylanisole + 4,6-Diiodo-2,3-dimethylanisole

Guidance literature:

With sulfuric acid; iodine; periodic acid; In acetic acid; at 80 - 85 ℃; for 12h;

DOI:10.1021/jo00129a041

upstream raw materials:

2,3-dimethylanisole

4-iodo-2,3-dimethyl-phenol

dimethyl sulfate

2,3-Dimethylphenol

Downstream raw materials:

Dimethyl-6-iod-3-methoxy-phthalat

5,6-dihydro-9-methoxy-6-methoxycarbonylmethyl-7,8-dimethyl-5-(4-methylbenzenesulfonyl)phenanthridine

3-methoxy-1,2-dimethyl-9-(4-methylbenzenesulfonyl)-9H-carbazole

3,4,2',3'-tetramethyl-5,4'-dimethoxy-2-(2-oxo-2-phenylethyl)-1,1'-biphenyl

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