N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide

Base Information

Chemical Name:N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide
CAS No.:1314258-29-1
Molecular Formula:C₂₂H₂₀N₄O₂S
Molecular Weight:404.492
Hs Code.:

Synonyms:N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide

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Chemical Property of N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide

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Technology Process of N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide

There total 6 articles about N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₄N₄O₃SSi

: 1314258-29-1
N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide

Guidance literature:: C₂₈H₃₄N₄O₃SSi; With trifluoroacetic acid; for 2h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield:

: 618-39-3
benzamidin

: 1314258-29-1
N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide / 20 h / 40 °C / Cooling with ice

2.1: sodium hydride / N,N-dimethyl-formamide; oil / 1 h / 20 °C / Cooling with ice

2.2: 1.5 h / Cooling with ice

3.1: bromine; sodium carbonate / dichloromethane; water / 0.67 h / 20 °C

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

5.1: trifluoroacetic acid / 2 h

With bromine; sodium hydride; sodium carbonate; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; oil;

Reference yield:

: 405554-88-3
4-(2-phenyl-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-imidazol-4-yl)pyridine

: 1314258-29-1
N-{3-[2-phenyl-4-(pyridin-4-yl)-1H-imidazol-5-yl]phenyl}ethane-1-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; sodium carbonate / dichloromethane; water / 0.67 h / 20 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

3: trifluoroacetic acid / 2 h

With bromine; sodium carbonate; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water;