{2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester

Base Information

Chemical Name:{2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester
CAS No.:1027046-69-0
Molecular Formula:C₁₁H₁₆ClN₃O₂
Molecular Weight:257.72
Hs Code.:

Synonyms:{2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester

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Chemical Property of {2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester

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Technology Process of {2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester

There total 4 articles about {2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026897-36-8
C₁₁H₁₄ClN₃O₃

: 1027046-69-0
{2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester

Guidance literature:: With acetic acid; zinc; In water; for 1h; Ambient temperature;
DOI:10.1021/jm960372b

Reference yield:

: 172462-31-6
(2-Hydroxy-1-methyl-ethyl)-carbamic acid methyl ester

: 1027046-69-0
{2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / oxalyl chloride, DMSO, Et₃N / CH₂Cl₂ / 1 h / -78 - 20 °C

2: NaBH₃CN / methanol / 16 h / Ambient temperature; pH 5-6

3: concd HCl, NaNO₂ / H₂O / 1 h / 0 °C

4: Zn (dust), acetic acid / H₂O / 1 h / Ambient temperature

With hydrogenchloride; oxalyl dichloride; sodium cyanoborohydride; acetic acid; dimethyl sulfoxide; triethylamine; zinc; sodium nitrite; In methanol; dichloromethane; water;
DOI:10.1021/jm960372b

Reference yield:

: 181881-57-2
(1-Methyl-2-oxo-ethyl)-carbamic acid methyl ester

: 1027046-69-0
{2-[N-(3-Chloro-phenyl)-hydrazino]-1-methyl-ethyl}-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₃CN / methanol / 16 h / Ambient temperature; pH 5-6

2: concd HCl, NaNO₂ / H₂O / 1 h / 0 °C

3: Zn (dust), acetic acid / H₂O / 1 h / Ambient temperature

With hydrogenchloride; sodium cyanoborohydride; acetic acid; zinc; sodium nitrite; In methanol; water;
DOI:10.1021/jm960372b