15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane

Base Information

• Chemical Name: 15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane
• CAS No.: 540522-39-2
• Molecular Formula: C₂₇H₃₃N₃O₂
• Molecular Weight: 431.578
• Mol file: 540522-39-2.mol

Synonyms:15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane

Chemical Property of 15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane

There total 3 articles about 15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

9-benzyl-8,9,10,11,19,20-hexahydro-5H,7H,13H-18,21-dioxa-6,9,12-triaza-dibenzo[a,g]cycloheptadecene-6,12-dicarboxylic acid di-tert-butyl ester → 15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane (540522-39-2)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 2h;

DOI:10.1071/CH02164

Reference yield:

benzyl chloride (100-44-7) → 15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane (540522-39-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / sodium carbonate / acetonitrile / 24 h / Heating

2: 93 percent / trifluoroacetic acid / 2 h / 20 °C

With sodium carbonate; trifluoroacetic acid; In acetonitrile;

DOI:10.1071/CH02164

Reference yield:

8,14-Bis(tert-butoxycarbonyl)-2,5-dioxa-8,11,14-triaza-1,6(1,2)-dibenzenacyclopentadecaphane (321658-92-8) → 15-benzyl-1,12,15-triaza-3,4:9,10-dibenzo-5,8-dioxacycloheptadecane (540522-39-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / sodium carbonate / acetonitrile / 24 h / Heating

2: 93 percent / trifluoroacetic acid / 2 h / 20 °C

With sodium carbonate; trifluoroacetic acid; In acetonitrile;

DOI:10.1071/CH02164

upstream raw materials:

benzyl chloride

8,14-Bis(tert-butoxycarbonyl)-2,5-dioxa-8,11,14-triaza-1,6(1,2)-dibenzenacyclopentadecaphane