C₇₅H₉₉IO₈Si

Base Information

Chemical Name:C₇₅H₉₉IO₈Si
CAS No.:864920-12-7
Molecular Formula:C₇₅H₉₉IO₈Si
Molecular Weight:1283.6
Hs Code.:

C<sub>75</sub>H<sub>99</sub>IO<sub>8</sub>Si

Synonyms:C₇₅H₉₉IO₈Si

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Chemical Property of C₇₅H₉₉IO₈Si

Chemical Property:

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Technology Process of C₇₅H₉₉IO₈Si

There total 8 articles about C₇₅H₉₉IO₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 864920-11-6
C₄₉H₅₆O₆Si

: 153033-34-2
1,4-bis(decyloxy)-2,5-diiodobenzene

: 864920-12-7
C₇₅H₉₉IO₈Si

Guidance literature:: With copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; triethylamine; at 20 ℃; for 1.25h; Inert atmosphere;
DOI:10.1039/c2cc30417a

Reference yield:

: 666837-02-1
C₂₈H₃₁BrO₆

: 864920-12-7
C₇₅H₉₉IO₈Si

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; triethylamine; triphenylphosphine / 6 h / 50 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran; methanol / 19 h / 20 °C

3: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine / 3 h / 50 °C / Inert atmosphere

4: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 20 °C

5: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; triethylamine / 1.25 h / 20 °C / Inert atmosphere

With copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1039/c2cc30417a

Reference yield:

: 29632-73-3
2-Bromo-4-iodoaniline

: 864920-12-7
C₇₅H₉₉IO₈Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; sodium nitrite / water / 0 °C

1.2: 1 h / 0 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 3 h / Inert atmosphere

3.1: iodine; methyl iodide / 12 h / 100 °C / Inert atmosphere

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1 h / 20 °C / Inert atmosphere

5.1: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine / 3 h / 50 °C / Inert atmosphere

6.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 20 °C

7.1: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; triethylamine / 1.25 h / 20 °C / Inert atmosphere

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; iodine; potassium carbonate; triethylamine; sodium nitrite; methyl iodide; In tetrahydrofuran; methanol; water;
DOI:10.1039/c2cc30417a