C₄₀H₇₀O₆Si₂

Base Information

Chemical Name:C₄₀H₇₀O₆Si₂
CAS No.:950598-31-9
Molecular Formula:C₄₀H₇₀O₆Si₂
Molecular Weight:703.163
Hs Code.:

C<sub>40</sub>H<sub>70</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₄₀H₇₀O₆Si₂

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Chemical Property of C₄₀H₇₀O₆Si₂

Chemical Property:

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Technology Process of C₄₀H₇₀O₆Si₂

There total 21 articles about C₄₀H₇₀O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 906624-11-1
(3S,6E)-8-(4-methoxybenzyloxy)-2,6-dimethylocta-1,6-dien-3-ol

: 950598-31-9
C₄₀H₇₀O₆Si₂

Guidance literature:: Multi-step reaction with 13 steps

1: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

2: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

3: DIBALH / CH₂Cl₂ / -78 °C

4: toluene / 80 °C

5: imidazole / CH₂Cl₂

6: DIBALH / CH₂Cl₂ / -78 °C

7: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

8: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

9: 63 percent / LDA / diethyl ether / -78 °C

10: imidazole / CH₂Cl₂

11: DIBALH / CH₂Cl₂ / -78 °C

12: toluene / 80 °C

13: DIBALH / CH₂Cl₂ / -78 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; 4 A molecular sieve; In diethyl ether; dichloromethane; toluene; 4: Wittig reaction / 7: Sharpless asymmetric epoxidation / 12: Wittig reaction;
DOI:10.1021/ja073952e

Reference yield:

: 906624-08-6
(2R,3S)-2-Iodomethyl-3-[(E)-5-(4-methoxy-benzyloxy)-3-methyl-pent-3-enyl]-2-methyl-oxirane

: 950598-31-9
C₄₀H₇₀O₆Si₂

Guidance literature:: Multi-step reaction with 14 steps

1: H₂O

2: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

3: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

4: DIBALH / CH₂Cl₂ / -78 °C

5: toluene / 80 °C

6: imidazole / CH₂Cl₂

7: DIBALH / CH₂Cl₂ / -78 °C

8: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

9: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

10: 63 percent / LDA / diethyl ether / -78 °C

11: imidazole / CH₂Cl₂

12: DIBALH / CH₂Cl₂ / -78 °C

13: toluene / 80 °C

14: DIBALH / CH₂Cl₂ / -78 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; water; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; 4 A molecular sieve; In diethyl ether; dichloromethane; toluene; 5: Wittig reaction / 8: Sharpless asymmetric epoxidation / 13: Wittig reaction;
DOI:10.1021/ja073952e

Reference yield:

: 950598-28-4
(3Z,5S,8E)-10-(4-methoxybenzyloxy)-4,8-dimethyldeca-3,8-dien-5-olide

: 950598-31-9
C₄₀H₇₀O₆Si₂

Guidance literature:: Multi-step reaction with 11 steps

1: DIBALH / CH₂Cl₂ / -78 °C

2: toluene / 80 °C

3: imidazole / CH₂Cl₂

4: DIBALH / CH₂Cl₂ / -78 °C

5: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

6: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

7: 63 percent / LDA / diethyl ether / -78 °C

8: imidazole / CH₂Cl₂

9: DIBALH / CH₂Cl₂ / -78 °C

10: toluene / 80 °C

11: DIBALH / CH₂Cl₂ / -78 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; 4 A molecular sieve; In diethyl ether; dichloromethane; toluene; 2: Wittig reaction / 5: Sharpless asymmetric epoxidation / 10: Wittig reaction;
DOI:10.1021/ja073952e