8-bromo-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone

Base Information

Chemical Name:8-bromo-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone
CAS No.:1159282-78-6
Molecular Formula:C₂₃H₂₇BrN₄O₆S
Molecular Weight:567.461
Hs Code.:

Synonyms:8-bromo-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-bromo-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone

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Technology Process of 8-bromo-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone

There total 1 articles about 8-bromo-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1159283-27-8
2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]amino-3-bromo-4,6-dimethoxybenzamide

: 1159282-78-6
8-bromo-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; for 4h; Reflux;
DOI:10.1016/j.bmcl.2009.03.125

Reference yield: 86.0%

: 1159282-78-6
8-bromo-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1159283-08-5
8-ethenyl-5,7-dimethoxy-2-[5-[(4-methyl-1-piperazinyl)sulfonyl]-2-ethoxybenzoyl]quinazolinone

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; cesium fluoride; In 1-methyl-pyrrolidin-2-one; at 50 ℃; for 4h;
DOI:10.1016/j.bmcl.2009.03.125