1,4-bis(3,4,5-trimethoxyphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

Base Information

Chemical Name:1,4-bis(3,4,5-trimethoxyphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene
CAS No.:404373-22-4
Molecular Formula:C₂₂H₂₈N₂O₆
Molecular Weight:416.474
Hs Code.:

Synonyms:1,4-bis(3,4,5-trimethoxyphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-bis(3,4,5-trimethoxyphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

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Technology Process of 1,4-bis(3,4,5-trimethoxyphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

There total 1 articles about 1,4-bis(3,4,5-trimethoxyphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 431-03-8
dimethylglyoxal

: 24313-88-0
3,4,5-Trimethoxyaniline

: 404373-22-4
1,4-bis(3,4,5-trimethoxyphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

Guidance literature:: With formic acid; In methanol; at 20 ℃;
DOI:10.1021/acs.macromol.8b01786

Reference yield: 90.0%

: bis[dimethyl(μ-dimethylsulfide)platinum(II)]

: 404373-22-4
1,4-bis(3,4,5-trimethoxyphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

: 404373-41-7
Pt(CH₃)2((OCH₃)3C₆H₂NCCH₃)2

Guidance literature:: In toluene; ligand and Pt-complex were added to flask, cooled to -78°C, evacuated, toluene was vac. transferred, warmed to room temp., stirred at room temp. for 3 nights under N2; toluene was removed in vacuo, petroleum ether was added, collected, washed with petroleum ether, dried for several h; elem. anal.;
DOI:10.1021/ja011189x