C₆₀H₆₂O₁₅

Base Information

• Chemical Name: C₆₀H₆₂O₁₅
• CAS No.: 1352561-86-4
• Molecular Formula: C₆₀H₆₂O₁₅
• Molecular Weight: 1023.14
• Mol file: 1352561-86-4.mol

Synonyms:C₆₀H₆₂O₁₅

Chemical Property of C₆₀H₆₂O₁₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₆₂O₁₅

There total 10 articles about C₆₀H₆₂O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

methyl 2,3,4-tri-O-benzyl-D-glucopyranoside (53008-65-4,641635-63-4) + C39H38O9S (1352561-52-4) → C60H62O15 (1352561-86-4)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; C₂₃H₂₅N₃O₆S; In dichloromethane; at -40 - 0 ℃; for 3h; Molecular sieve;

DOI:10.1021/jo201586r

Reference yield:

methyl 2,3,4-tri-O-benzyl-D-glucopyranoside (53008-65-4,641635-63-4) + C30H32O7S (1352561-50-2) + C39H38O9S (1352561-52-4) → C51H56O13 (1352561-84-2) + C60H62O15 (1352561-86-4)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -40 - 0 ℃; for 3h; Molecular sieve;

DOI:10.1021/jo201586r

Reference yield:

C38H34O7S → C60H62O15 (1352561-86-4)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 °C

3: dmap; diisopropyl-carbodiimide / dichloromethane / 20 °C

4: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 3 h / -40 - 0 °C / Molecular sieve

With dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; water; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jo201586r

upstream raw materials:

p-methylphenyl 4,6-O-benzylidine-3-O-(naphthalen-2-ylmethyl)-1-thio-β-D-glucopyranoside

methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

C₃₀H₃₂O₇S

C₃₉H₃₈O₉S