<1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate

Base Information

Chemical Name:<1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate
CAS No.:185515-93-9
Molecular Formula:C₁₉H₂₅NO₄
Molecular Weight:331.412
Hs Code.:

Synonyms:<1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate

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Chemical Property of <1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate

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Technology Process of <1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate

There total 5 articles about <1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 185515-94-0
<1R-(1α,2β,5α)>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-3-nitropropanoate

: 185515-93-9
<1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate

Guidance literature:: With methanesulfonyl chloride; triethylamine; at 0 ℃; for 0.116667h;
DOI:10.1039/CC9960002543

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 185515-93-9
<1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / Et₃N, DMAP / CH₂Cl₂ / 0.08 h / 0 °C

2: 100 percent / aq. NaIO₄, OsO₄ / dioxane / 2 h

3: 91 percent / neutral alumina / 1.) 0 deg C, 0.5 h, 2.) r.t., 3 h

4: 90 percent / MsCl, Et₃N / 0.12 h / 0 °C

With dmap; aluminum oxide; sodium periodate; osmium(VIII) oxide; methanesulfonyl chloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1039/CC9960002543

Reference yield:

: 72526-00-2
(-)-8-phenylmenthyl acrylate

: 185515-93-9
<1R-<1α(E),2β,5α>>-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 3-nitro-2-propenoate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / aq. NaIO₄, OsO₄ / dioxane / 2 h

2: 91 percent / neutral alumina / 1.) 0 deg C, 0.5 h, 2.) r.t., 3 h

3: 90 percent / MsCl, Et₃N / 0.12 h / 0 °C

With aluminum oxide; sodium periodate; osmium(VIII) oxide; methanesulfonyl chloride; triethylamine; In 1,4-dioxane;
DOI:10.1039/CC9960002543