cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide

Base Information

Chemical Name:cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide
CAS No.:1594113-00-4
Molecular Formula:C₃₆H₃₇BrNiP₂
Molecular Weight:670.231
Hs Code.:

Synonyms:cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide

Chemical Property:

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Technology Process of cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide

There total 3 articles about cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 15629-93-3
[1,3-bis(diphenylphosphino)propane]nickel(II) bromide

: 2633-66-1
2-mesitylmagnesium bromide

: 1594113-00-4
cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide

Guidance literature:: In tetrahydrofuran; dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1021/om500156q

Reference yield: 85.0%

: 1594113-00-4
cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 0.25h;

Reference yield:

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: 1594113-00-4
cis-[1,3-bis(diphenylphosphino)propane](2,4,6-trimethylphenyl)nickel(II) bromide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 0.5 h / 80 °C / Sealed tube; Inert atmosphere

2: dichloromethane; tetrahydrofuran / 0.25 h / 0 °C

In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/om500156q