tetraphenyldiphosphoxanetriphenylphosphine chlororhodium(I)(tetrahydrofuran) 1:1

Base Information

Chemical Name:tetraphenyldiphosphoxanetriphenylphosphine chlororhodium(I)(tetrahydrofuran) 1:1
CAS No.:136595-85-2
Molecular Formula:C₄H₈O*C₄₂H₃₅ClOP₃Rh
Molecular Weight:859.126
Hs Code.:

Synonyms:tetraphenyldiphosphoxanetriphenylphosphine chlororhodium(I)(tetrahydrofuran) 1:1

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Chemical Property of tetraphenyldiphosphoxanetriphenylphosphine chlororhodium(I)(tetrahydrofuran) 1:1

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Technology Process of tetraphenyldiphosphoxanetriphenylphosphine chlororhodium(I)(tetrahydrofuran) 1:1

There total 6 articles about tetraphenyldiphosphoxanetriphenylphosphine chlororhodium(I)(tetrahydrofuran) 1:1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 14694-95-2
Wilkinson's catalyst

: 124191-07-7
Diphenylphosphino propenoate

: 136595-85-2
tetraphenyldiphosphoxanetriphenylphosphine chlororhodium(I)(tetrahydrofuran) 1:1

Guidance literature:: With P(C₆H₅)3; In tetrahydrofuran; under N2, 0°C, 1.2 h stirring; filtration, reduction of vol., standing at 3°C for several days, drying in vac., elem. anal.;
DOI:10.1039/DT9910001765

Reference yield: 64.0%

: 14694-95-2
Wilkinson's catalyst

: 124191-07-7
Diphenylphosphino propenoate

: 136595-85-2
tetraphenyldiphosphoxanetriphenylphosphine chlororhodium(I)(tetrahydrofuran) 1:1

: tris(triphenylphosphine)(triphenylphosphoniopropionate)rhodium(I) hexafluorophosphate-tetrahydrofuran (1/1)

Guidance literature:: With TlPF₆; In tetrahydrofuran; byproducts: TlCl; under N2, 0°C, soln. obtained after filtration of (RhCl(PPh3)(Ph2POPPh2)) was treated with TlPF6, 1 h stirring at 0°C, fine white ppt. of TlCl was allowed to settle; soln. was filtered and evapd., standing for 3°C for 1 d, ppt. was collected, dried in vac., elem. anal.;
DOI:10.1039/DT9910001765