1,1-diiodo-2,3,4,5-tetraphenylstannole

Base Information

Chemical Name:1,1-diiodo-2,3,4,5-tetraphenylstannole
CAS No.:77904-13-3
Molecular Formula:C₂₈H₂₀I₂Sn
Molecular Weight:728.986
Hs Code.:

Synonyms:1,1-diiodo-2,3,4,5-tetraphenylstannole

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Chemical Property of 1,1-diiodo-2,3,4,5-tetraphenylstannole

Chemical Property:

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Technology Process of 1,1-diiodo-2,3,4,5-tetraphenylstannole

There total 2 articles about 1,1-diiodo-2,3,4,5-tetraphenylstannole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 21813-34-3
hexaphenylstannol

: 77904-13-3
1,1-diiodo-2,3,4,5-tetraphenylstannole

Guidance literature:: With iodine; In tetrachloromethane; byproducts: iodobenzene; under N2, addn. of soln. of iodine to soln. of complex at 0°C, 2h, stirring; removed the solvent in vac., dissolved in methylene chloride, filtered,pptd. by addn. of ethanol and cooling with dry ice; elem. anal.;
DOI:10.1021/ja00404a024

Reference yield:

: 21289-08-7,99643-57-9
1,4-dilithio-1,2,3,4-tetraphenylbutadiene

: 77904-13-3
1,1-diiodo-2,3,4,5-tetraphenylstannole

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether

2: iodine / tetrachloromethane

With iodine; In tetrahydrofuran; tetrachloromethane; diethyl ether;
DOI:10.1021/ja00404a024

Reference yield: 79.0%

: 66-71-7
1,10-Phenanthroline

: 77904-13-3
1,1-diiodo-2,3,4,5-tetraphenylstannole

: 77904-32-6
1,1-diiodo-2,3,4,5-tetraphenylstannole 1,10-phenanthroline adduct

Guidance literature:: In diethyl ether; benzene; benzene soln. of Sn compd. was treated with Et2O soln. of ligand; stirring at room temp. for 30 min (N2); evapn., treatment with benzene, filtration, cooling; elem. anal.;
DOI:10.1021/ic50224a060