4-OXO-2,2,6,6-TETRAMETHYLPIPERIDINE-D16,1-15N-1-OXYL

Base Information

Chemical Name:4-OXO-2,2,6,6-TETRAMETHYLPIPERIDINE-D16,1-15N-1-OXYL
CAS No.:80404-14-4
Molecular Formula:C₉H₁₆NO₂
Molecular Weight:187.098
Hs Code.:
Mol file:80404-14-4.mol

Synonyms:4-Oxo-2,2,6,6-tetramethylpiperidine-d16,1-15N-1-oxyl;4-oxo-2,2,6,6-tetra((2)H3)methyl-1-(3,3,5,5-(2)H4,1-(15)N)piperidinyloxyl;4-oxo-2,2,6,6-tetramethylpiperidine-d16;4-Oxo-TEMPO-d16,1-15N,free radical;TEMPONE-1-15N;TEMPONE-d16,1-15N;1-15N-1-oxyl;4-Oxo-TEMPO-1-15N;

Suppliers and Price of 4-OXO-2,2,6,6-TETRAMETHYLPIPERIDINE-D16,1-15N-1-OXYL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
4-Oxo-TEMPO-d16,15N, free radical 98 atom %
100mg
$ 609.00

Medical Isotopes, Inc.
4-Oxo-2,2,6,6-tetramethylpiperidine-d16,1-15N-1-oxyl
50 mg
$ 490.00

American Custom Chemicals Corporation
4-OXO-TEMPO-D16,1-15N, FREE RADICAL 95.00%
100MG
$ 994.46

Total 8 raw suppliers

Chemical Property of 4-OXO-2,2,6,6-TETRAMETHYLPIPERIDINE-D16,1-15N-1-OXYL

Chemical Property:

Melting Point:35oC(lit.)
PSA：20.31000
LogP:1.49190
Storage Temp.:0-6°C

Purity/Quality:

99.90% ^*data from raw suppliers

4-Oxo-TEMPO-d16,15N, free radical 98 atom % ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 4-Oxo-2,2,6,6-tetramethylpiperidine-d16;1-15N-1-oxyl (CAS# 80404-14-4) is a useful isotopically labeled research compound.

Technology Process of 4-OXO-2,2,6,6-TETRAMETHYLPIPERIDINE-D16,1-15N-1-OXYL

There total 3 articles about 4-OXO-2,2,6,6-TETRAMETHYLPIPERIDINE-D16,1-15N-1-OXYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.1%

: 61431-36-5
4-oxo-2,2,6,6-tetra(²H₃)methyl-(3,3,5,5-(²H₄),1-¹⁵N)piperidine

: 80404-14-4
4-oxo-2,2,6,6-tetramethylpiperidine-d16, 1-¹⁵N-1-oxyl

Guidance literature:: With sodium tungstate (VI) dihydrate; dihydrogen peroxide; In water; at 5 - 25 ℃;
DOI:10.1002/ardp.200800053

Reference yield:

: 80404-11-1
4-oxo-2,2,6,6-tetra(²H₃)methyl-(3,3,5,5-²H₄,1-¹⁵N)piperidine

: 80404-14-4
4-oxo-2,2,6,6-tetramethylpiperidine-d16, 1-¹⁵N-1-oxyl

Guidance literature:: With sodium tungstate; Na₄EDTA; hydrogen peroxide; In water-d2; for 240h; Darkness;
DOI:10.1021/jo1011619

Reference yield:

: 4-oxo-2,2,6,6-tetra(⁽²⁾H₃)methyl-1-(⁽²⁾H)hydroxy-(3,3,5,5-⁽²⁾H₄,1-⁽¹⁵⁾N)piperidine ⁽²⁾H-hydrochloride

: 3-bromo-4-oxo-2,2,6,6-tetra(²H₃)methyl-1-(3,5,5-²H₃,1-¹⁵N)piperidinyloxyl

: 80404-14-4
4-oxo-2,2,6,6-tetramethylpiperidine-d16, 1-¹⁵N-1-oxyl

Guidance literature:: 4-oxo-2,2,6,6-tetra(⁽²⁾H₃)methyl-1-(⁽²⁾H)hydroxy-(3,3,5,5-⁽²⁾H₄,1-⁽¹⁵⁾N)piperidine ⁽²⁾H-hydrochloride; With bromine; In chloroform; at 20 ℃; for 2.5h;

With sodium nitrite; In water-d2; chloroform; for 0.25h;
DOI:10.1021/jo1011619