(S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal

Base Information

Chemical Name:(S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal
CAS No.:1009643-89-3
Molecular Formula:C₁₉H₂₇NO₃
Molecular Weight:317.428
Hs Code.:

Synonyms:(S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal

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Chemical Property of (S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal

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Technology Process of (S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal

There total 3 articles about (S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5153-67-3
nitrostyrene

: 112-45-8
10-Undecenal

: 1009643-89-3
(S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal

: 1262281-23-1
(R)-2-((S)-2-nitro-1-phenylethyl)undec-10-enal

Guidance literature:: 10-Undecenal; With (S)-2-[(S)-2,2-diphenyl-1,3-dioxolan-4-yl]pyrrolidine; In methyl cyclohexane; at 20 ℃; for 0.166667h;

nitrostyrene; In methyl cyclohexane; at 20 ℃; for 70h; Overall yield = 100 %Spectr.;
DOI:10.3762/bjoc.13.59

Reference yield:

: 112-45-8
10-Undecenal

: 102-96-5
(2-nitroethenyl)benzene

: 1009643-89-3
(S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal

: 2-(2-nitro-1-phenylethyl)undec-10-enal

Guidance literature:: With benzoic acid; In water; at 0 - 20 ℃; Title compound not separated from byproducts.;
DOI:10.1002/anie.200704161

Reference yield:

: 112-45-8
10-Undecenal

: 102-96-5
(2-nitroethenyl)benzene

: 1009643-89-3
(S)-2-((R)-2-nitro-1-phenylethyl)undec-10-enal

: 1262281-23-1
(R)-2-((S)-2-nitro-1-phenylethyl)undec-10-enal

Guidance literature:: With magnetic nanoparticles (Fe₃O₄ coated with SiO₂)-supported (S)-diphenylprolinol trimethylsilyl ether catalyst; In ethanol; water; at 20 ℃; for 48h; optical yield given as %ee; diastereoselective reaction;
DOI:10.1002/adsc.201000508