4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.0^2,11.0^3,10.0^4,6.0^7,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester

Base Information

• Chemical Name: 4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.0^2,11.0^3,10.0^4,6.0^7,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester
• CAS No.: 86814-76-8
• Molecular Formula: C₃₂H₃₄N₂O₆
• Molecular Weight: 542.632

Synonyms:4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.0^2,11.0^3,10.0^4,6.0^7,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester

Chemical Property of 4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.0^2,11.0^3,10.0^4,6.0^7,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester

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Technology Process of 4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.0^2,11.0^3,10.0^4,6.0^7,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester

There total 4 articles about 4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.0^2,11.0^3,10.0^4,6.0^7,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

4,7-Dimethyl-15-oxo-5,6-diphenyl-11,12-diazapentacyclo<8.2.2.14,7.02,9.03,8>pentadeca-5,13-dien-11,12-dicarbonsaeure-diethylester (73240-57-0,77881-55-1) → diethyl hydrazodicarboxylate (4114-28-7) + methyl 3',6'-dimethyl[1,1*:2',1-terphenyl]-4'-carboxylate (13102-23-3) + 4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.02,11.03,10.04,6.07,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester (86814-76-8) + diethylazodicarboxylate (1972-28-7,218603-74-8)

Guidance literature:

In diethyl ether; acetone; at -25 - -20 ℃; for 6h; Irradiation;

Reference yield: 46.0%

4,7-Dimethyl-15-oxo-5,6-diphenyl-11,12-diazapentacyclo<8.2.2.14,7.02,9.03,8>pentadeca-5,13-dien-11,12-dicarbonsaeure-diethylester (73240-57-0,77881-55-1) → diethyl hydrazodicarboxylate (4114-28-7) + methyl 3',6'-dimethyl[1,1*:2',1-terphenyl]-4'-carboxylate (13102-23-3) + 4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.02,11.03,10.04,6.07,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester (86814-76-8) + diethylazodicarboxylate (1972-28-7,218603-74-8) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1)

Guidance literature:

In diethyl ether; acetone; at -25 - -20 ℃; for 6h; Product distribution; Irradiation;

Reference yield: 9.0%

4,7-Dimethyl-5,6-diphenyl-11,12-diazatetracyclo<8.2.2.02,9.03,8>tetradeca-4,6,13-trien-11,12-dicarbonsaeure-diethylester (86814-77-9) → methyl 3',6'-dimethyl[1,1*:2',1-terphenyl]-4'-carboxylate (13102-23-3) + 4,7-Dimethyl-5,6-diphenyl-11,12-diazatetracyclo<8.2.2.02,9.03,8>tetradeca-3,5,7,13-tetraen-11,12-dicarbonsaeure-diethylester (86814-78-0) + 4,9-Dimethyl-6,7-diphenyl-5,8-dioxa-13,14-diazahexacyclo<10.2.2.02,11.03,10.04,6.07,9>hexadec-15-en-13,14-dicarbonsaeure-diethylester (86814-76-8)

Guidance literature:

With oxygen; methylene blue; In dichloromethane; for 5h; Irradiation;

upstream raw materials:

4,7-Dimethyl-15-oxo-5,6-diphenyl-11,12-diazapentacyclo<8.2.2.1^4,7.0^2,9.0^3,8>pentadeca-5,13-dien-11,12-dicarbonsaeure-diethylester

4,7-Dimethyl-5,6-diphenyl-11,12-diazatetracyclo<8.2.2.0^2,9.0^3,8>tetradeca-4,6,13-trien-11,12-dicarbonsaeure-diethylester

(1R,2R,5S,6S)-7,8-Diaza-tricyclo[4.2.2.0^2,5]deca-3,9-diene-7,8-dicarboxylic acid diethyl ester

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