AcNHPhDN

Base Information

Chemical Name:AcNHPhDN
CAS No.:1294513-59-9
Molecular Formula:C₁₆H₁₇NO
Molecular Weight:239.317
Hs Code.:

Synonyms:AcNHPhDN

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Chemical Property of AcNHPhDN

Chemical Property:

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Technology Process of AcNHPhDN

There total 7 articles about AcNHPhDN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1294513-58-8
mDNOTf

: 78887-39-5
3-Acetamidophenylboronic acid

: 1294513-59-9
AcNHPhDN

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; for 2h; Inert atmosphere; Reflux;

Reference yield:

: 1165952-91-9
cyclohexa-1,3-diene

: 1294513-59-9
AcNHPhDN

Guidance literature:: Multi-step reaction with 4 steps

1.1: 3,5-dibutyl-4-hydroxytoluene / 40 h / 70 °C / Inert atmosphere

2.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; oxygen / dichloromethane; water / 40 h / 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 48 h / 20 °C

4.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 2 h / Inert atmosphere; Reflux

With 3,5-dibutyl-4-hydroxytoluene; oxygen; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium hydroxide; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 4.1: Suzuki Coupling;

Reference yield:

: 40610-12-6
Bicyclo<2.2.2>oct-5-ene-2-carboxylic acid

: 1294513-59-9
AcNHPhDN

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / N,N,N,N,N,N-hexamethylphosphoric triamide; tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide dimethyl acetal / dichloromethane / 12 h / -78 - 20 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 48 h / 20 °C

4.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 2 h / Inert atmosphere; Reflux

With sodium hydrogencarbonate; N,N-dimethyl-formamide dimethyl acetal; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; toluene; 4.1: Suzuki Coupling;