(S,E)-methyl 2-(N-ethyl-N-(4-methoxyphenyl)amino)-2-(naphthalen-2-yl)-5-phenylpent-4-enoate

Base Information

Chemical Name:(S,E)-methyl 2-(N-ethyl-N-(4-methoxyphenyl)amino)-2-(naphthalen-2-yl)-5-phenylpent-4-enoate
CAS No.:1586007-56-8
Molecular Formula:C₃₁H₃₁NO₃
Molecular Weight:465.592
Hs Code.:

Synonyms:(S,E)-methyl 2-(N-ethyl-N-(4-methoxyphenyl)amino)-2-(naphthalen-2-yl)-5-phenylpent-4-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,E)-methyl 2-(N-ethyl-N-(4-methoxyphenyl)amino)-2-(naphthalen-2-yl)-5-phenylpent-4-enoate

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Technology Process of (S,E)-methyl 2-(N-ethyl-N-(4-methoxyphenyl)amino)-2-(naphthalen-2-yl)-5-phenylpent-4-enoate

There total 1 articles about (S,E)-methyl 2-(N-ethyl-N-(4-methoxyphenyl)amino)-2-(naphthalen-2-yl)-5-phenylpent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21040-45-9
Cinnamyl acetate

: 1586007-48-8
(Z)-methyl 2-(4-methoxyphenylimino)-2-(naphthalen-2-yl)acetate

: 925-90-6
ethylmagnesium bromide

: 1586007-56-8
(S,E)-methyl 2-(N-ethyl-N-(4-methoxyphenyl)amino)-2-(naphthalen-2-yl)-5-phenylpent-4-enoate

: (R,E)-methyl 2-(N-ethyl-N-(4-methoxyphenyl)amino)-2-(naphthalen-2-yl)-5-phenylpent-4-enoate

Guidance literature:: (Z)-methyl 2-(4-methoxyphenylimino)-2-(naphthalen-2-yl)acetate; ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Inert atmosphere; Schlenk technique;

Cinnamyl acetate; With (R)-(-)-5,5’-bis(diphenyl;phosphine)-2,2,2’,2’-tetrafluoro-4,4’-bi-1,3-benzodioxole; bis(η3-allyl-μ-chloropalladium(II)); In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Overall yield = 72 %; Overall yield = 89 mg; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol500506t