methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Base Information

Chemical Name:methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate
CAS No.:1391908-85-2
Molecular Formula:C₂₂H₁₈N₂O₄
Molecular Weight:374.396
Hs Code.:

Synonyms:methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

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Chemical Property of methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Chemical Property:

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Technology Process of methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

There total 9 articles about methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1391908-79-4
methyl (R)-[1-(benzoyloxy)-2-iodoethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

: 1391908-85-2
methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 10h;
DOI:10.1002/ejoc.201200235

Reference yield:

: 1042149-39-2
methyl (S)-1-(1,2-dihydroxyethyl)-9H-pyrido[3,4-b]indole-3-carboxylate

: 1391908-85-2
methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / dichloromethane / 5.33 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / chloroform / 0.25 h / 0 °C

3: N-ethyl-N,N-diisopropylamine / chloroform / 4 h / 50 °C

4: hydrogenchloride / water; acetonitrile / 4 h / 20 °C

5: triethylamine / dichloromethane / 0.17 h / 0 °C

6: sodium iodide / acetone / Reflux; Inert atmosphere

7: palladium 10% on activated carbon; hydrogen / ethyl acetate / 10 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; In dichloromethane; chloroform; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1002/ejoc.201200235

Reference yield:

: C₃₅H₃₀N₂O₆S

: 1391908-85-2
methyl (S)-1-[1-(benzoyloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / chloroform / 4 h / 50 °C

2: hydrogenchloride / water; acetonitrile / 4 h / 20 °C

3: triethylamine / dichloromethane / 0.17 h / 0 °C

4: sodium iodide / acetone / Reflux; Inert atmosphere

5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 10 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; In dichloromethane; chloroform; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1002/ejoc.201200235