C₃₀H₃₆O₅Si

Base Information

Chemical Name:C₃₀H₃₆O₅Si
CAS No.:1360932-61-1
Molecular Formula:C₃₀H₃₆O₅Si
Molecular Weight:504.698
Hs Code.:

C<sub>30</sub>H<sub>36</sub>O<sub>5</sub>Si

Synonyms:C₃₀H₃₆O₅Si

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Chemical Property of C₃₀H₃₆O₅Si

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Technology Process of C₃₀H₃₆O₅Si

There total 5 articles about C₃₀H₃₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 107-86-8
3,3-dimethyl acrylaldehyde

: 1360932-59-7
C₂₅H₂₈O₄Si

: 1360932-61-1
C₃₀H₃₆O₅Si

Guidance literature:: With (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid; In toluene; at 20 ℃; for 88h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/chem.201102192

Reference yield:

: 1132-21-4
3,5-dimethoxybenzoic acid

: 1360932-61-1
C₃₀H₃₆O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 1 h / 0 °C

3.2: 3 h / 20 °C

4.1: aluminum (III) chloride; sodium iodide / dichloromethane; acetonitrile / 1 h / 0 °C

5.1: (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid / toluene / 88 h / 20 °C

With 1H-imidazole; aluminum (III) chloride; lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201102192

Reference yield:

: 705-76-0
3,5-dimethoxybenzyl alcohol

: 1360932-61-1
C₃₀H₃₆O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 1 h / 0 °C

2.2: 3 h / 20 °C

3.1: aluminum (III) chloride; sodium iodide / dichloromethane; acetonitrile / 1 h / 0 °C

4.1: (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid / toluene / 88 h / 20 °C

With 1H-imidazole; aluminum (III) chloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201102192