C₆₀H₆₆O₂SSi

Base Information

Chemical Name:C₆₀H₆₆O₂SSi
CAS No.:775306-60-0
Molecular Formula:C₆₀H₆₆O₂SSi
Molecular Weight:879.334
Hs Code.:

C<sub>60</sub>H<sub>66</sub>O<sub>2</sub>SSi

Synonyms:C₆₀H₆₆O₂SSi

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Chemical Property of C₆₀H₆₆O₂SSi

Chemical Property:

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Technology Process of C₆₀H₆₆O₂SSi

There total 4 articles about C₆₀H₆₆O₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 606098-82-2
1,4-bis(hexyloxy)-2-ethynyl-5-(2-triisopropylsilylethynyl)benzene

: 775306-57-5
C₂₉H₁₇BrS

: 775306-60-0
C₆₀H₆₆O₂SSi

Guidance literature:: With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 50 ℃; for 8h;
DOI:10.1021/ma048728d

Reference yield:

: C₂₄H₁₇Br₂O⁽¹⁺⁾*BF₄^(1-)

: 775306-60-0
C₆₀H₆₆O₂SSi

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / acetic anhydride / 2 h / 150 °C

2: 28 percent / PdCl₂(PPh₃)2; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-acetamide / 12 h / 160 °C

3: 97 percent / N-bromosuccinimide; acetic acid / CHCl₃ / Heating

4: 64 percent / Pd(PPh₃)4; CuI; piperidine / tetrahydrofuran / 8 h / 50 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic anhydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; chloroform; N,N-dimethyl acetamide;
DOI:10.1021/ma048728d

Reference yield:

: 775306-53-1
C₂₉H₁₈S

: 775306-60-0
C₆₀H₆₆O₂SSi

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / N-bromosuccinimide; acetic acid / CHCl₃ / Heating

2: 64 percent / Pd(PPh₃)4; CuI; piperidine / tetrahydrofuran / 8 h / 50 °C

With piperidine; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; In tetrahydrofuran; chloroform;
DOI:10.1021/ma048728d