2'-methyl-4-amino-4'-nitrodiphenyl sulfone

Base Information

Chemical Name:2'-methyl-4-amino-4'-nitrodiphenyl sulfone
CAS No.:176512-38-2
Molecular Formula:C₂₃H₂₃BrN₂O₆S₂
Molecular Weight:567.481
Hs Code.:

2'-methyl-4-<N-(3-bromopropyl)-N-tosyl>amino-4'-nitrodiphenyl sulfone

Synonyms:2'-methyl-4-amino-4'-nitrodiphenyl sulfone

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Chemical Property of 2'-methyl-4-amino-4'-nitrodiphenyl sulfone

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Technology Process of 2'-methyl-4-amino-4'-nitrodiphenyl sulfone

There total 4 articles about 2'-methyl-4-amino-4'-nitrodiphenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 176512-30-4
4-amino-2'-methyl-4'-nitrodiphenyl sulfide

: 176512-38-2
2'-methyl-4-amino-4'-nitrodiphenyl sulfone

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 65 ℃;
DOI:10.1002/ardp.19963290309

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 176512-38-2
2'-methyl-4-amino-4'-nitrodiphenyl sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3 h

2: 79 percent / NaI, CuI, aq. KOH / ethanol / 17 h / Heating

3: 94 percent / 30percent H₂O₂ / acetic acid / 65 °C

With potassium hydroxide; copper(l) iodide; dihydrogen peroxide; sodium iodide; In pyridine; ethanol; acetic acid;
DOI:10.1002/ardp.19963290309

Reference yield:

: 4-(2-Methyl-4-nitro-phenylsulfanyl)-phenylamine

: 176512-38-2
2'-methyl-4-amino-4'-nitrodiphenyl sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3 h

2: 79 percent / NaI, CuI, aq. KOH / ethanol / 17 h / Heating

3: 94 percent / 30percent H₂O₂ / acetic acid / 65 °C

With potassium hydroxide; copper(l) iodide; dihydrogen peroxide; sodium iodide; In pyridine; ethanol; acetic acid;
DOI:10.1002/ardp.19963290309