ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate

Base Information

Chemical Name:ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate
CAS No.:139944-74-4
Molecular Formula:C₂₄H₃₆O₅
Molecular Weight:404.547
Hs Code.:

Synonyms:ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate

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Chemical Property of ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate

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Technology Process of ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate

There total 3 articles about ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 139944-73-3
ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methyl-3-pentynedioate

: 139944-74-4
ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate

Guidance literature:: With hydrogen; Lindlar's catalyst; In methanol; for 5h; under 760 Torr; Ambient temperature;
DOI:10.1021/jo00036a034

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 139944-74-4
ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent

3: 95 percent / H₂ / Lindlar catalyst / methanol / 5 h / 760 Torr / Ambient temperature

With hydrogen; Lindlar's catalyst; In methanol;
DOI:10.1021/jo00036a034

Reference yield:

: 88292-41-5
2-Oxopropansaeure-<(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl>ester

: 139944-74-4
ethyl 5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-2-methylpentanedioate

Guidance literature:: Multi-step reaction with 2 steps

2: 95 percent / H₂ / Lindlar catalyst / methanol / 5 h / 760 Torr / Ambient temperature

With hydrogen; Lindlar's catalyst; In methanol;
DOI:10.1021/jo00036a034