1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone

Base Information

Chemical Name:1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone
CAS No.:161181-86-8
Molecular Formula:C₂₁H₂₆N₂O₄
Molecular Weight:370.448
Hs Code.:

1-<4-(tert-butyloxycarbonyl)phenyl>-4-<cyano(ethoxycarbonyl)methylene>piperidinone

Synonyms:1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone

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Technology Process of 1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone

There total 1 articles about 1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 95017-68-8
1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone

: 105-56-6
ethyl 2-cyanoacetate

: 161181-86-8
1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone

Guidance literature:: With ammonium acetate; acetic acid; In benzene; for 6h; Heating;
DOI:10.1002/jhet.5570310522

Reference yield: 100.0%

: 161181-86-8
1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone

: 161181-87-9
1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 2h; under 2689.2 Torr;
DOI:10.1002/jhet.5570310522

Reference yield:

: 161181-86-8
1-<4-(tert-butyloxycarbonyl)phenyl>-4-piperidinone

: 4-(2,4-diamino-6(5H)-oxopyrimidin-5-yl)-1-(4-carboxyphenyl)piperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / 10percent Pd/C / ethanol / 2 h / 2689.2 Torr

2: 1.) C₂H₅ONa / 1.) EtOH, reflux, 30 min, 2.) EtOH, reflux, 23 h

3: 74 percent / trifluoroacetic acid / 2 h / 0 °C

With hydrogen; sodium ethanolate; trifluoroacetic acid; palladium on activated charcoal; In ethanol;
DOI:10.1002/jhet.5570310522