C₃₄H₄₆N₄O₉

Base Information

Chemical Name:C₃₄H₄₆N₄O₉
CAS No.:1221741-79-2
Molecular Formula:C₃₄H₄₆N₄O₉
Molecular Weight:654.761
Hs Code.:

C<sub>34</sub>H<sub>46</sub>N<sub>4</sub>O<sub>9</sub>

Synonyms:C₃₄H₄₆N₄O₉

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Chemical Property of C₃₄H₄₆N₄O₉

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Technology Process of C₃₄H₄₆N₄O₉

There total 8 articles about C₃₄H₄₆N₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1221741-77-0
C₄₃H₆₆N₄O₉Si

: 1221741-79-2
C₃₄H₄₆N₄O₉

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ol1006696

Reference yield:

: 1360566-51-3
C₂₄H₄₀N₂O₆Si

: 1221741-79-2
C₃₄H₄₆N₄O₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / -40 °C

1.2: 5 h / -40 - 0 °C

2.1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

3.1: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

4.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

5.1: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

With hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; tetrabutyl ammonium fluoride; sodium acetate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058

Reference yield:

: 1221741-69-0
C₂₄H₄₂N₂O₅Si

: 1221741-79-2
C₃₄H₄₆N₄O₉

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

2: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

3: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

With hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; tetrabutyl ammonium fluoride; sodium acetate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058