HYDROCINNAMIC-D9 ACID

Base Information

Chemical Name:HYDROCINNAMIC-D9 ACID
CAS No.:93131-15-8
Molecular Formula:C₉H₁₀O₂
Molecular Weight:159.106
Hs Code.:
Mol file:93131-15-8.mol

Synonyms:HYDROCINNAMIC-D9 ACID;3-Phenylpropionic-d9 acid;Hydrocinnamic acid-d9,OH

Suppliers and Price of HYDROCINNAMIC-D9 ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Medical Isotopes, Inc.
Hydrocinnamic-d9Acid
5 g
$ 1650.00

American Custom Chemicals Corporation
HYDROCINNAMIC ACID-D9,OH 95.00%
5G
$ 1388.60

American Custom Chemicals Corporation
HYDROCINNAMIC ACID-D9,OH 95.00%
1G
$ 788.29

Total 7 raw suppliers

Chemical Property of HYDROCINNAMIC-D9 ACID

Chemical Property:

Melting Point:47-49 °C(lit.)
Boiling Point:280 °C(lit.)
Flash Point:113 °C
PSA：37.30000
LogP:1.70380
Storage Temp.:-20°C Freezer, Under inert atmosphere
Solubility.:Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

Hydrocinnamic-d9Acid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:: SDS file from LookChem

Useful:

Uses Hydrocinnamic-d9 Acid (CAS# 93131-15-8) is a useful isotopically labeled research compound.

Technology Process of HYDROCINNAMIC-D9 ACID

There total 1 articles about HYDROCINNAMIC-D9 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18509-03-0
sodium trans-cinnamate

: 93131-15-8
2,2,3,3,2',3',4',5',6'-nonadeuterophenylpropanic acid

Guidance literature:: With deuterated Raney nickel; In water-d2; at 70 ℃; for 18h; Product distribution; deuteration/reduction of carbonyl compopunds and aromatic nucleus;
DOI:10.1016/S0040-4039(01)81217-X

Reference yield:

: 93131-15-8
2,2,3,3,2',3',4',5',6'-nonadeuterophenylpropanic acid

: C₁₆H₇⁽²⁾H₈N

Guidance literature:: Multi-step reaction with 4 steps

1: polyphosphoric acid / 3.5 h / 70 °C

2: toluene-4-sulfonic acid / toluene / 3 h / Reflux

3: sodium tetrahydroborate; deuteroacetic acid / tetrahydrofuran / 1.5 h / 0 °C

4: lead(IV) tetraacetate / deuteromethanol / 0.5 h / 0 °C

With sodium tetrahydroborate; deuteroacetic acid; lead(IV) tetraacetate; toluene-4-sulfonic acid; In tetrahydrofuran; deuteromethanol; toluene;
DOI:10.1016/j.tetlet.2011.02.033

Reference yield:

: 93131-15-8
2,2,3,3,2',3',4',5',6'-nonadeuterophenylpropanic acid

: C₃₄H₂₆⁽²⁾H₈N₆O₅S

Guidance literature:: Multi-step reaction with 7 steps

1: polyphosphoric acid / 3.5 h / 70 °C

2: toluene-4-sulfonic acid / toluene / 3 h / Reflux

3: sodium tetrahydroborate; deuteroacetic acid / tetrahydrofuran / 1.5 h / 0 °C

4: lead(IV) tetraacetate / deuteromethanol / 0.5 h / 0 °C

5: hydrogen chloride / ethyl [2]alcohol; water-d2 / 18 h / 95 °C

6: N-ethyl-N,N-diisopropylamine / iso-butanol / 4.5 h / 150 °C / Microwave irradiation

7: triethylamine / 1 h / 0 °C

With sodium tetrahydroborate; deuteroacetic acid; lead(IV) tetraacetate; hydrogen chloride; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; deuteromethanol; ethyl [2]alcohol; water-d2; toluene; iso-butanol;
DOI:10.1016/j.tetlet.2011.02.033