ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate

Base Information

Chemical Name:ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate
CAS No.:1357380-97-2
Molecular Formula:C₂₃H₂₆N₈O₅
Molecular Weight:494.51
Hs Code.:

Synonyms:ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate

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Chemical Property of ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate

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Technology Process of ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate

There total 6 articles about ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1357380-83-6
C₁₈H₁₈N₈O₃

: 1357380-97-2
ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate

Guidance literature:: With potassium hydroxide; In water; dimethyl sulfoxide; at 20 ℃;
DOI:10.1002/hlca.201100189

Reference yield:

: 58-55-9,75448-53-2
theophylline

: 1357380-97-2
ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; potassium carbonate / N,N-dimethyl-formamide / Reflux

2: copper(l) iodide / tetrahydrofuran; water / Reflux

3: potassium hydroxide / water; dimethyl sulfoxide / 20 °C

With copper(l) iodide; tetrabutylammomium bromide; potassium carbonate; potassium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 2: Huisgen cycloaddition;
DOI:10.1002/hlca.201100189

Reference yield:

: 14114-45-5
N-propargyltheophylline

: 1357380-97-2
ethyl 2-{{{(1Z)-1-phenyl-2-{4-[ (2,3,6,7-tetrahydro-1,3-dimethyl-2,6-dioxo-1H-purin-7-yl)methyl]-1H-1,2,3-triazol-1-yl}ethylidene}amino}oxy}propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide / tetrahydrofuran; water / Reflux

2: potassium hydroxide / water; dimethyl sulfoxide / 20 °C

With copper(l) iodide; potassium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide; 1: Huisgen cycloaddition;
DOI:10.1002/hlca.201100189