p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate

Base Information

Chemical Name:p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate
CAS No.:312264-06-5
Molecular Formula:C₂₁H₂₅NOTe
Molecular Weight:435.036
Hs Code.:

Synonyms:p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate

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Chemical Property of p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate

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Technology Process of p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate

There total 3 articles about p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 312263-99-3
p-methylphenyl 3-methyltellurobutanoate

: 312264-06-5
p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate

Guidance literature:: In water; at 100 ℃; for 12h;
DOI:10.1016/S0040-4039(00)01287-9

Reference yield:

: 32294-57-8
bis(4-methylphenyl)ditelluride

: 312264-06-5
p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / NaBH₄ / tetrahydrofuran; ethanol / 3 h

2: 87 percent / H₂O / 12 h / 100 °C / UV-irradiation

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; water;
DOI:10.1021/ja003879r

Reference yield:

: 108-12-3
isopentanoyl chloride

: 312264-06-5
p-methylphenyl N-(2,6-dimethylphenyl)-4-methyl-2-oxotelluropentyro-imidate

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / NaBH₄ / tetrahydrofuran; ethanol / 3 h

2: 87 percent / H₂O / 12 h / 100 °C / UV-irradiation

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; water;
DOI:10.1021/ja003879r