4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene

Base Information

• Chemical Name: 4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene
• CAS No.: 190788-99-9
• Molecular Formula: C₅₉H₇₆N₄OP₂
• Molecular Weight: 919.226

Synonyms:4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene

Chemical Property of 4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene

Chemical Property:

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Technology Process of 4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene

There total 1 articles about 4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

4,5-bis(diethoxyphosphonito)-9,9-dimethylxanthene → 4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene (190788-99-9)

Guidance literature:

4,5-bis(diethoxyphosphonito)-9,9-dimethylxanthene; With n-butyllithium; In tetrahydrofuran; hexane; at -45 ℃; for 0.5h; Inert atmosphere;

4,5-bis(diethoxyphosphonito)-9,9-dimethylxanthene; In tetrahydrofuran; hexane; at -65 - 20 ℃; Inert atmosphere;

DOI:10.1002/asia.201100092

Reference yield: 100.0%

hydridocarbonyltris(triphenylphosphine)rhodium(I) + 4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene (190788-99-9) → HRh(4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene)(CO)(PPh3) (190789-39-0)

Guidance literature:

In benzene-d6; Ar-atmosphere; stirring (25°C, overnight);

DOI:10.1021/om970068w

Reference yield:

4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene (190788-99-9) → 4,5-bis(bis{p-[(diethylammonium chloride)methyl]phenyl}phosphino)-9,9-dimethylxanthene tetrahydrochloride

Guidance literature:

With hydrogenchloride; In diethyl ether;

DOI:10.1002/asia.201100092

Downstream raw materials:

Rh(4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene)(CO)(acac)

HRh(4,6-bis[bis(4-((diethylamino)methyl)phenyl)phosphino]-10,10-dimethylxanthene)(CO)(PPh₃)

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