C₃₄H₅₂O₇Si

Base Information

Chemical Name:C₃₄H₅₂O₇Si
CAS No.:1268268-90-1
Molecular Formula:C₃₄H₅₂O₇Si
Molecular Weight:600.868
Hs Code.:

C<sub>34</sub>H<sub>52</sub>O<sub>7</sub>Si

Synonyms:C₃₄H₅₂O₇Si

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Chemical Property of C₃₄H₅₂O₇Si

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Technology Process of C₃₄H₅₂O₇Si

There total 13 articles about C₃₄H₅₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₅₂O₆Si

: 1268268-90-1
C₃₄H₅₂O₇Si

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water; In tert-butyl alcohol; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja200089f

Reference yield:

: 1268268-84-3
C₂₄H₂₈O₄

: 1268268-90-1
C₃₄H₅₂O₇Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: 3,3-dimethyldioxirane / dichloromethane / -78 - 0 °C / Inert atmosphere

1.2: 1.17 h / -78 - 0 °C / Inert atmosphere

1.3: 0 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

3.1: diethyl ether; toluene / 0.67 h / -78 - 0 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / methanol / 3 h / 65 °C / Inert atmosphere

6.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

6.2: 0.5 h / -78 - 20 °C / Inert atmosphere

7.1: copper(l) iodide / tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

7.2: 2 h / -40 °C / Inert atmosphere

8.1: camphor-10-sulfonic acid / methanol / 1 h / 0 - 20 °C / Inert atmosphere

9.1: potassium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

9.2: 5 h / 0 - 20 °C / Inert atmosphere

10.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran; tert-butyl alcohol / 16 h / 20 °C / Inert atmosphere

11.1: lead(IV) tetraacetate / benzene / 1 h / 20 °C / Inert atmosphere

12.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; copper(l) iodide; osmium(VIII) oxide; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; camphor-10-sulfonic acid; water; lead(IV) tetraacetate; 3,3-dimethyldioxirane; pyridinium p-toluenesulfonate; potassium hydride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; mineral oil; tert-butyl alcohol; benzene;
DOI:10.1021/ja200089f

Reference yield:

: C₂₈H₃₆O₄

: 1268268-90-1
C₃₄H₅₂O₇Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride

2.1: 3,3-dimethyldioxirane / dichloromethane / -78 - 0 °C / Inert atmosphere

2.2: 1.17 h / -78 - 0 °C / Inert atmosphere

2.3: 0 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

4.1: diethyl ether; toluene / 0.67 h / -78 - 0 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / methanol / 3 h / 65 °C / Inert atmosphere

7.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

7.2: 0.5 h / -78 - 20 °C / Inert atmosphere

8.1: copper(l) iodide / tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

8.2: 2 h / -40 °C / Inert atmosphere

9.1: camphor-10-sulfonic acid / methanol / 1 h / 0 - 20 °C / Inert atmosphere

10.1: potassium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

10.2: 5 h / 0 - 20 °C / Inert atmosphere

11.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran; tert-butyl alcohol / 16 h / 20 °C / Inert atmosphere

12.1: lead(IV) tetraacetate / benzene / 1 h / 20 °C / Inert atmosphere

13.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; copper(l) iodide; osmium(VIII) oxide; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; camphor-10-sulfonic acid; water; lead(IV) tetraacetate; 3,3-dimethyldioxirane; pyridinium p-toluenesulfonate; potassium hydride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; mineral oil; tert-butyl alcohol; benzene;
DOI:10.1021/ja200089f