m-(Phenylsulfonyl)benzoic acid

Base Information

• Chemical Name: m-(Phenylsulfonyl)benzoic acid
• CAS No.: 2548-44-9
• Molecular Formula: C₁₃H₁₀O₄S
• Molecular Weight: 262.286
• Hs Code.: 2916399090
• Mol file: 2548-44-9.mol

Synonyms:Benzoicacid, m-(phenylsulfonyl)- (6CI,7CI,8CI);NSC43055;m-Phenylsulfonylbenzoic acid;

Chemical Property of m-(Phenylsulfonyl)benzoic acid

Chemical Property:

• Vapor Pressure: 4.45E-11mmHg at 25°C
• Refractive Index: 1.616
• Boiling Point: 506.4 °C at 760 mmHg
• Flash Point: 260.1 °C
• PSA: 79.82000
• Density: 1.378 g/cm³
• LogP: 3.29840

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of m-(Phenylsulfonyl)benzoic acid

There total 17 articles about m-(Phenylsulfonyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyldiphenylsulphone (5402-35-7) → 3-benzenesulfonyl-benzoic acid (2548-44-9)

Guidance literature:

With chromium(VI) oxide; acetic acid;

DOI:10.1021/ja01151a012

Reference yield:

3-methylphenylsulfonyl chloride (1899-93-0) → 3-benzenesulfonyl-benzoic acid (2548-44-9)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃

2: CrO₃; acetic acid

With chromium(VI) oxide; aluminium trichloride; acetic acid;

DOI:10.1021/ja01151a012

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 3-benzenesulfonyl-benzoic acid (2548-44-9)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃

2: CrO₃; acetic acid

With chromium(VI) oxide; aluminium trichloride; acetic acid;

DOI:10.1021/ja01151a012

upstream raw materials:

3-methyldiphenylsulphone

3-(phenylthio)benzoic acid

<3-Methoxycarbonyl-phenyl>-phenyl-sulfon

3-Carboxybenzenesulfonyl chloride