3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline

Base Information

Chemical Name:3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline
CAS No.:1027509-93-8
Molecular Formula:C₂₀H₁₉ClN₄O₃
Molecular Weight:398.849
Hs Code.:

Synonyms:3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline

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Chemical Property of 3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline

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Technology Process of 3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline

There total 7 articles about 3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 149156-05-8
3-chloro-2-nitro-N-formylaniline

: 141815-91-0
1-(3-chloropropyl)-5-methyl-4-phenylimidazole

: 1027509-93-8
3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline

Guidance literature:: With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 3h;
DOI:10.1021/jm00063a013

Reference yield:

: 19088-99-4
3-chloro-2-nitrobenzoyl chloride

: 1027509-93-8
3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline

Guidance literature:: Multi-step reaction with 5 steps

1: NaN₃ / acetone; H₂O / 0.5 h / Ambient temperature

2: benzene / Heating

3: 5 N aq. NaOH / benzene / 1 h / Ambient temperature

4: 81 percent / 1 h / Heating

5: 50 percent / NaI, K₂CO₃ / dimethylformamide / 3 h / 60 °C

With sodium hydroxide; sodium azide; potassium carbonate; sodium iodide; In water; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/jm00063a013

Reference yield:

: 4771-47-5
3-chloro-2-nitro-benzoic acid

: 1027509-93-8
3-chloro-2-nitro-N-formyl-N-<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>aniline

Guidance literature:: Multi-step reaction with 6 steps

1: SOCl₂ / 3 h / Heating

2: NaN₃ / acetone; H₂O / 0.5 h / Ambient temperature

3: benzene / Heating

4: 5 N aq. NaOH / benzene / 1 h / Ambient temperature

5: 81 percent / 1 h / Heating

6: 50 percent / NaI, K₂CO₃ / dimethylformamide / 3 h / 60 °C

With sodium hydroxide; thionyl chloride; sodium azide; potassium carbonate; sodium iodide; In water; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/jm00063a013