(3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxamide

Base Information

• Chemical Name: (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxamide
• CAS No.: 1025366-72-6
• Molecular Formula: C₄₃H₄₉N₅O₉S
• Molecular Weight: 811.956

Synonyms:(3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxamide

Chemical Property of (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxamide

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Technology Process of (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxamide

There total 1 articles about (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pent-4-en-1-yl [(1S)-1-({(2S,4R)-2-{[((1R,2S)-1-{[(cyclopropylsulfonyl)amino]-carbonyl}-2-vinylcyclopropyl)amino]carbonyl}-4-[(7-methoxy-2-phenyl-6-vinylquinolin-4-yl)oxy]pyrrolidin-1-yl}carbonyl)oct-7-en-1-yl]carbamate (1025370-16-4) → (3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1(35),12,26,28,30,31,33,35-octaene-9-carboxamide (1025366-72-6)

Guidance literature:

Zhan catalyst 1B; In 1,2-dichloro-ethane; at 90 ℃; for 3.5h;

Reference yield:

(3R,6S,9R,11S,12Z,19S,26E)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1(35),12,26,28,30,31,33,35-octaene-9-carboxamide (1025366-72-6) → (3R,6S,9R,11R,12Z,19S)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1(35),28,30,31,33,35-hexaene-9-carboxamide (1025366-77-1)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; for 15h;

upstream raw materials:

pent-4-en-1-yl [(1S)-1-({(2S,4R)-2-{[((1R,2S)-1-{[(cyclopropylsulfonyl)amino]-carbonyl}-2-vinylcyclopropyl)amino]carbonyl}-4-[(7-methoxy-2-phenyl-6-vinylquinolin-4-yl)oxy]pyrrolidin-1-yl}carbonyl)oct-7-en-1-yl]carbamate

Downstream raw materials:

(3R,6S,9R,11R,12Z,19S)-N-(cyclopropylsulfonyl)-29-methoxy-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,28,30,31,33,35-hexaene-9-carboxamide

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