7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde

Base Information

Chemical Name:7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde
CAS No.:1372129-89-9
Molecular Formula:C₄₅H₄₅N₃O₃S₃
Molecular Weight:772.069
Hs Code.:

Synonyms:7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde

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Chemical Property of 7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde

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Technology Process of 7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde

There total 6 articles about 7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1071224-34-4
7-bromobenzo[c][1,2,5]thiadiazole-4-carboxaldehyde

: 1372129-88-8
5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-5'-(tri-n-butylstannyl)-2,2'-bithiophene

: 1372129-89-9
7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde

Guidance literature:: With bis(triphenylphosphine)palladium(II)-chloride; In tetrahydrofuran; at 70 ℃; for 15h; Inert atmosphere;
DOI:10.1002/adfm.201102519

Reference yield: 71.0%

: 1071224-34-4
7-bromobenzo[c][1,2,5]thiadiazole-4-carboxaldehyde

: 1421265-53-3
C₄₁H₅₁NO₂S₂Sn

: 1372129-89-9
7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2012.12.071

Reference yield:

: 2255-78-9
4-bromo-7-(bromomethyl)benzo[c][1,2,5]thiadiazole

: 1372129-89-9
7-(5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-2,2'-bithien-5'-yl)benzo[c]-[1,2,5]thiadiazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / 1,4-dioxane; water / 1 h / Reflux

2: manganese(IV) oxide / chloroform / 19 h / 20 °C / Reflux

3: bis(triphenylphosphine)palladium(II)-chloride / tetrahydrofuran / 15 h / 70 °C / Inert atmosphere

With manganese(IV) oxide; bis(triphenylphosphine)palladium(II)-chloride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; chloroform; water;
DOI:10.1002/adfm.201102519