Technology Process of C29H31N5O3
There total 10 articles about C29H31N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-Bromosuccinimide / acetonitrile / 2 h / 20 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C
3: dmap; triethylamine / dichloromethane / 3 h / 20 °C
4: N,N-dimethyl-formamide / 0.5 h / 20 °C
5: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium phosphate / tetrahydrofuran / 2 h / 120 °C / Inert atmosphere; Microwave irradiation
6: trifluoroacetic acid / dichloromethane
With
dmap; potassium phosphate; N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C
2: dmap; triethylamine / dichloromethane / 3 h / 20 °C
3: N,N-dimethyl-formamide / 0.5 h / 20 °C
4: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium phosphate / tetrahydrofuran / 2 h / 120 °C / Inert atmosphere; Microwave irradiation
5: trifluoroacetic acid / dichloromethane
With
dmap; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;