bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)

Base Information

Chemical Name:bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)
CAS No.:1448998-05-7
Molecular Formula:C₅₈H₄₃N₃O₄P₂Pt
Molecular Weight:1103.02
Hs Code.:

bis(triphenylphosphine)(η<sup>2</sup>-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)

Synonyms:bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)

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Chemical Property of bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)

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Technology Process of bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)

There total 3 articles about bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 12120-15-9
ethylenebis(triphenylphosphine)platinum⁽⁰⁾

: 9-diazofluoren-1-yl 4-nitrocinnamate

: 1448998-05-7
bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)

Guidance literature:: In benzene; for 1h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1016/j.jorganchem.2013.04.045

Reference yield:

: 1448998-06-8
N'-(1-hydroxy-9H-fluoren-9-ylidene)-4-methylbenzenesulfonohydrazide

: 1448998-05-7
bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 - 20 °C / Inert atmosphere; Schlenk technique; Glovebox

1.2: 1 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

2.1: sodium hydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere; Schlenk technique; Glovebox

2.2: 0.75 h / 75 °C / Inert atmosphere; Schlenk technique; Glovebox

3.1: benzene / 1 h / Inert atmosphere; Schlenk technique; Glovebox

With sodium hydride; In tetrahydrofuran; benzene;
DOI:10.1016/j.jorganchem.2013.04.045

Reference yield:

: 9-(2-tosylhydrazono)fluoren-1-yl 4-nitrocinnamate

: 1448998-05-7
bis(triphenylphosphine)(η²-9-diazofluoren-1-yl-4-nitrocinnamate)platinum(0)

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere; Schlenk technique; Glovebox

1.2: 0.75 h / 75 °C / Inert atmosphere; Schlenk technique; Glovebox

2.1: benzene / 1 h / Inert atmosphere; Schlenk technique; Glovebox

With sodium hydride; In tetrahydrofuran; benzene;
DOI:10.1016/j.jorganchem.2013.04.045