3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine

Base Information

Chemical Name:3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine
CAS No.:151143-07-6
Molecular Formula:C₂₆H₃₀ClNO₄
Molecular Weight:455.982
Hs Code.:

Synonyms:3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine

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Chemical Property of 3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine

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Technology Process of 3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine

There total 3 articles about 3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 151143-03-2
3-bromomethyl-6-chloro-5-ethyl-2-methoxypyridine

: sodium 1,3-dibenzyloxy-2-propanolate

: 151143-07-6
3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine

Guidance literature:: In tetrahydrofuran; for 7h; Heating;
DOI:10.1016/S0040-4020(01)89920-8

Reference yield:

: 125849-98-1
3,5-dichloro-6-ethyl-2H-1,4-oxazin-2-one

: 151143-07-6
3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / HCl / 0.25 h / 0 °C

2: 82 percent / toluene / 90 °C

3: 72 percent / tetrahydrofuran / 7 h / Heating

With hydrogenchloride; In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(01)89920-8

Reference yield:

: 151143-01-0
5-chloro-6-ethyl-3-methoxy-2H-1,4-oxazin-2-one

: 151143-07-6
3-<1,3-(dibenzyloxy-2-propoxy)methyl>-6-chloro-2-methoxy-5-ethylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / toluene / 90 °C

2: 72 percent / tetrahydrofuran / 7 h / Heating

In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(01)89920-8