4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

Base Information

Chemical Name:4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside
CAS No.:1021496-21-8
Molecular Formula:C₆₆H₇₄Cl₃NO₁₅
Molecular Weight:1227.67
Hs Code.:

4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

Synonyms:4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

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Chemical Property of 4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

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Technology Process of 4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

There total 1 articles about 4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1021496-22-9
ethyl 2,4-di-O-benzyl-3-deoxy-1-thio-3-(2,2,2-trichloroethoxycarbonylamino)-β-D-fucopyranoside

: 1021496-46-7
4-methoxyphenyl 3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

: 1021496-21-8
4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

Guidance literature:: With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; In diethyl ether; dichloromethane; at -20 ℃; for 1.5h;
DOI:10.1016/j.tet.2008.01.093

Reference yield: 86.0%

: 1021496-21-8
4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

: 1021496-49-0
4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

Guidance literature:: palladium dichloride; In methanol; dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2008.01.093

Reference yield:

: 1021496-21-8
4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

: 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-β-D-rhamnopyranose

: 1021496-53-6
2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranose

Guidance literature:: With ammonium cerium(IV) nitrate; In water; toluene; acetonitrile; at 20 ℃; Title compound not separated from byproducts.;
DOI:10.1016/j.tet.2008.01.093