tert-butyl 2-(9-(3-(3-(trifluoromethyl)-3H-diazirine-3-yl)benzyl)-9H-carbazol-2-yloxy)-acetate

Base Information

• Chemical Name: tert-butyl 2-(9-(3-(3-(trifluoromethyl)-3H-diazirine-3-yl)benzyl)-9H-carbazol-2-yloxy)-acetate
• CAS No.: 1204407-35-1
• Molecular Formula: C₂₇H₂₄F₃N₃O₃
• Molecular Weight: 495.501

Synonyms:tert-butyl 2-(9-(3-(3-(trifluoromethyl)-3H-diazirine-3-yl)benzyl)-9H-carbazol-2-yloxy)-acetate

Chemical Property of tert-butyl 2-(9-(3-(3-(trifluoromethyl)-3H-diazirine-3-yl)benzyl)-9H-carbazol-2-yloxy)-acetate

Chemical Property:

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Technology Process of tert-butyl 2-(9-(3-(3-(trifluoromethyl)-3H-diazirine-3-yl)benzyl)-9H-carbazol-2-yloxy)-acetate

There total 1 articles about tert-butyl 2-(9-(3-(3-(trifluoromethyl)-3H-diazirine-3-yl)benzyl)-9H-carbazol-2-yloxy)-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

tert-butyl 2-(9H-carbazol-2-yloxy)acetate (210410-32-5) + 3-[3'-(bromomethyl)phenyl]-3-(trifluoromethyl)-3H-diazirine (162845-02-5) → tert-butyl 2-(9-(3-(3-(trifluoromethyl)-3H-diazirine-3-yl)benzyl)-9H-carbazol-2-yloxy)-acetate (1204407-35-1)

Guidance literature:

tert-butyl 2-(9H-carbazol-2-yloxy)acetate; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

3-[3'-(bromomethyl)phenyl]-3-(trifluoromethyl)-3H-diazirine; In tetrahydrofuran; at 0 - 20 ℃; Darkness;

DOI:10.1016/j.bmcl.2009.10.035

Reference yield: 76.0%

tert-butyl 2-(9-(3-(3-(trifluoromethyl)-3H-diazirine-3-yl)benzyl)-9H-carbazol-2-yloxy)-acetate (1204407-35-1) → BSc3958 (1204407-34-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1016/j.bmcl.2009.10.035

upstream raw materials:

tert-butyl 2-(9H-carbazol-2-yloxy)acetate

3-[3'-(bromomethyl)phenyl]-3-(trifluoromethyl)-3H-diazirine

Downstream raw materials:

BSc₃₉₅₈

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