2-acetylphenyl thiophene-2-carboxylate

Base Information

Chemical Name:2-acetylphenyl thiophene-2-carboxylate
CAS No.:77708-28-2
Molecular Formula:C₁₃H₁₀O₃S
Molecular Weight:246.287
Hs Code.:

Synonyms:2-acetylphenyl thiophene-2-carboxylate

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Chemical Property of 2-acetylphenyl thiophene-2-carboxylate

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-acetylphenyl thiophene-2-carboxylate

There total 4 articles about 2-acetylphenyl thiophene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 5271-67-0
2-Thiophenecarbonyl chloride

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 77708-28-2
2-acetylphenyl thiophene-2-carboxylate

Guidance literature:: With pyridine; at 25 ℃; Cooling with ice;
DOI:10.1039/b9nj00237e

Reference yield: 60.0%

: 527-72-0
2-thiophenylcarboxylic acid

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 77708-28-2
2-acetylphenyl thiophene-2-carboxylate

Guidance literature:: With pyridine; trichlorophosphate; for 2h;

Reference yield:

: 527-72-0
2-thiophenylcarboxylic acid

: 77708-28-2
2-acetylphenyl thiophene-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: potassium hydroxide / methanol / Inert atmosphere

2.2: 0.08 h / 20 °C / Inert atmosphere

With oxalyl dichloride; N,N-dimethyl-formamide; potassium hydroxide; In methanol; dichloromethane;
DOI:10.1039/d0ob01783c