TETRAMETHYL(N-PROPYL)CYCLOPENTADIENE

Base Information

• Chemical Name: TETRAMETHYL(N-PROPYL)CYCLOPENTADIENE
• CAS No.: 64417-12-5
• Molecular Formula: C₁₂H₂₀
• Molecular Weight: 164.291
• Mol file: 64417-12-5.mol

Synonyms:TETRAMETHYL(N-PROPYL)CYCLOPENTADIENE;Tetramethyl-(propyl)-cyclopentadiene;n-Propyl(tetramethylcyclopentadiene);Tetramethyl(n-propyl)cyclopentadiene, min. 97%

Chemical Property of TETRAMETHYL(N-PROPYL)CYCLOPENTADIENE

Chemical Property:

• Vapor Pressure: 0.326mmHg at 25°C
• Refractive Index: n20/D 1.474
• Boiling Point: 207.3 °C at 760 mmHg
• Flash Point: 67.9 °C
• PSA: 0.00000
• Density: 0.816 g/cm³
• LogP: 4.08910
• Storage Temp.: 2-8°C

Purity/Quality:

99.5% ^*data from raw suppliers

Tetramethyl(n-propyl)cyclopentadiene, min. 97% ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TETRAMETHYL(N-PROPYL)CYCLOPENTADIENE

There total 3 articles about TETRAMETHYL(N-PROPYL)CYCLOPENTADIENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2E,5E)-3,5-Dimethyl-4-propyl-hepta-2,5-dien-4-ol → ligand C5Me4HCH2CH2CH3 (64417-12-5)

Guidance literature:

With toluene-4-sulfonic acid; In diethyl ether;

DOI:10.1016/S0022-328X(00)87959-0

Reference yield:

2,3,4,5-tetramethyl-2-cyclopenten-1-one (54458-61-6) → ligand C5Me4HCH2CH2CH3 (64417-12-5)

Guidance literature:

Multi-step reaction with 2 steps

2: I₂

With iodine;

Reference yield:

2,3,4,5-Tetramethyl-1-propyl-cyclopent-2-enol → ligand C5Me4HCH2CH2CH3 (64417-12-5) + tetramethyl(n-propyl)cyclopentadiene (83321-20-4) + 1,2,3-Trimethyl-4-methylene-5-propyl-cyclopentene

Guidance literature:

With iodine; Title compound not separated from byproducts;

upstream raw materials:

2,3,4,5-tetramethyl-2-cyclopenten-1-one

Downstream raw materials:

[η⁵-C₅Me₄(n-propyl)]₂Mo₂(CO)₆

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