2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose

Base Information

Chemical Name:2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose
CAS No.:1632073-34-7
Molecular Formula:C₆₃H₆₉IO₁₀Si
Molecular Weight:1141.22
Hs Code.:

Synonyms:2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose

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Chemical Property of 2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose

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Technology Process of 2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose

There total 1 articles about 2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1326706-59-5
6'-O-(tert-butyldiphenyl)silyl-2,3,3',4,4'-penta-O-benzylsucrose

: 1632073-34-7
2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose

: 1632073-35-8
2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-1’,6-dideoxy-1’,6-di-iodosucrose

Guidance literature:: 6'-O-(tert-butyldiphenyl)silyl-2,3,3',4,4'-penta-O-benzylsucrose; With triphenylphosphine; In toluene; for 0.333333h; Reflux;

With 1H-imidazole; iodine; In toluene; for 2h; Reflux;
DOI:10.1055/s-0033-1340180

Reference yield: 96.0%

: 1632073-34-7
2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose

: 1632073-37-0
6-azido-6-deoxy-2,3,3’,4,4’-Penta-O-benzyl-6’-O-tert-butyldiphenylsilylsucrose

Guidance literature:: With sodium azide; tetrabutylammomium bromide; In N,N-dimethyl-formamide; at 80 ℃; for 2h;
DOI:10.1055/s-0033-1340180

Reference yield:

: 1632073-34-7
2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-6-O-deoxy-6-iodosucrose

: 1632073-38-1
6-azido-6-deoxy-2,3,3’,4,4’-penta-O-benzyl-6’-O-tert-butyldiphenylsilyl-1’-O-(prop-2-en-1-yl)sucrose

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C

2: tetrabutylammomium bromide; sodium hydroxide / toluene; water / 10 h / 20 °C

With sodium azide; tetrabutylammomium bromide; sodium hydroxide; In water; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-0033-1340180